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Research Containing: Temperature

Correction of the equilibrium temperature caused by slight evaporation of water in protein crystal growth cells during long-term space experiments at International Space Station

by on 22 August 2016in Biology & Biotechnology, Physical Sciences

The normal growth rates of the {110} faces of tetragonal hen egg-white lysozyme crystals, R, were measured as a function of the supersaturation sigma parameter using a reflection type interferometer under muG at the International Space Station (NanoStep Project). Since water slightly evaporated from in situ observation cells during a long-term space station experiment for several months, equilibrium temperature T(e) changed, and the actual sigma, however, significantly increased mainly due to the increase in salt concentration C(s). To correct sigma, the actual C(s) and protein concentration C(p), which correctly represent the measured T(e) value in space, were first calculated. Second, a new solubility curve with the corrected C(s) was plotted. Finally, the revised sigma was obtained from the new solubility curve. This correction method successfully revealed that the 2.8% water was evaporated from the solution, leading to 2.8% increase in the C(s) and C(p) of the solution.

Related URLs:
http://www.ncbi.nlm.nih.gov/pubmed/26329200

MISSE 1 and 2 Tray Temperature measurements

by on 9 June 2015in Technology Development & Demonstration No comment

The Materials International Space Station Experiment (MISSE 1 & 2) was deployed August 10, 2001 and retrieved July 30, 2005. This experiment is a co-operative endeavor by NASA-LaRC, NASA-GRC, NASA MSFC, NASA-JSC, the Materials Laboratory at the Air Force Research Laboratory, and the Boeing Phantom Works. The objective of the experiment is to evaluate performance, stability, and long term survivability of materials and components planned for use by NASA and DOD on future LEO, synchronous orbit, and interplanetary space missions. Temperature is an important parameter in the evaluation of space environmental effects on materials. The MISSE 1 & 2 had autonomous temperature data loggers to measure the temperature of each of the four experiment trays. The MISSE tray-temperature data loggers have one external thermistor data channel, and a 12 bit digital converter. The MISSE experiment trays were exposed to the ISS space environment for nearly four times the nominal design lifetime for this experiment. Nevertheless, all of the data loggers provided useful temperature measurements of MISSE. The temperature measurement system has been discussed in a previous paper. This paper presents temperature measurements of MISSE payload experiment carriers (PECs) 1 and 2 experiment trays.

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 Investigation on mechanism of faceted cellular array growth in International Space Station

by on 9 June 2015in Physical Sciences No comment

An in situ observation experiment of faceted cellular growth was carried out using transparent organic alloy, salol – t-butyl alcohol, in microgravity conditions on the International Space Station. The temperature and solute concentration fields in the vicinity of the solid-liquid and the growth rate were simultaneously measured by microscopic interferometers.

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Measurements of the neutron dose and energy spectrum on the International Space Station during expeditions ISS-16 to ISS-21

by on 9 June 2015in Physical Sciences No comment

As part of the international Matroshka-R and Radi-N experiments, bubble detectors have been used on board the ISS in order to characterise the neutron dose and the energy spectrum of neutrons. Experiments using bubble dosemeters inside a tissue-equivalent phantom were performed during the ISS-16, ISS-18 and ISS-19 expeditions. During the ISS-20 and ISS-21 missions, the bubble dosemeters were supplemented by a bubble-detector spectrometer, a set of six detectors that was used to determine the neutron energy spectrum at various locations inside the ISS. The temperature-compensated spectrometer set used is the first to be developed specifically for space applications and its development is described in this paper. Results of the dose measurements indicate that the dose received at two different depths inside the phantom is not significantly different, suggesting that bubble detectors worn by a person provide an accurate reading of the dose received inside the body. The energy spectra measured using the spectrometer are in good agreement with previous measurements and do not show a strong dependence on the precise location inside the station. To aid the understanding of the bubble-detector response to charged particles in the space environment, calculations have been performed using a Monte-Carlo code, together with data collected on the ISS. These calculations indicate that charged particles contribute <2% to the bubble count on the ISS, and can therefore be considered as negligible for bubble-detector measurements in space.

Related URLs:
http://www.ncbi.nlm.nih.gov/pubmed/22826353

SUBSA and PFMI Transparent Furnace Systems Currently in use in the International Space Station Microgravity Science Glovebox

by on 9 June 2015in Physical Sciences No comment

The Solidification Using a Baffle in Sealed Ampoules (SUBSA) and Pore Formation and Mobility Investigation (PFMI) furnaces were developed for operation in the International Space Station (ISS) Microgravity Science Glovebox (MSG). Both furnaces were launched to the ISS on STS-111, June 4, 2002, and are currently in use on orbit. The SUBSA furnace provides a maximum temperature of 850 C and can accommodate a metal sample as large as 30 cm long and 12mm in diameter. SUBSA utilizes a gradient freeze process with a minimum cooldown rate of 0.5C per min, and a stability of +/- 0.15C. An 8 cm long transparent gradient zone coupled with a Cohu 3812 camera and quartz ampoule allows for observation and video recording of the solidification process. PFMI is a Bridgman type furnace that operates at a maximum temperature of 130C and can accommodate a sample 23cm long and 10mm in diameter. Two Cohu 3812 cameras mounted 90 deg apart move on a separate translation system which allows for viewing of the sample in the transparent hot zone and gradient zone independent of the furnace translation rate and direction. Translation rates for both the cameras and furnace can be specified from 0.5micrometers/sec to 100 micrometers/sec with a stability of +/-5%. The two furnaces share a Process Control Module (PCM) which controls the furnace hardware, a Data Acquisition Pad (DaqPad) which provides signal condition of thermal couple data, and two Cohu 3812 cameras. The hardware and software allow for real time monitoring and commanding of critical process control parameters. This paper will provide a detailed explanation of the SUBSA and PFMI systems along with performance data and some preliminary results from completed on-orbit processing runs.

Related URLs:
http://dx.doi.org/10.2514/6.2003-1362

Limits to gelation in colloidal aggregation

by on 9 June 2015in Physical Sciences No comment

We show that the dynamics of large fractal colloid aggregates are well described by a combination of translational and rotational diffusion and internal elastic fluctuations, allowing both the aggregate size and internal elasticity to be determined by dynamic light scattering. The comparison of results obtained in microgravity and on Earth demonstrates that cluster growth is limited by gravity-induced restructuring. In the absence of gravity, thermal fluctuations ultimately inhibit fractal growth and set the fundamental limitation to the lowest volume fraction which will gel.

Related URLs:
http://www.ncbi.nlm.nih.gov/pubmed/15447462

Analysis of the Thermal Performance of SODI Instrument for DCMIX Configuration

by on 9 June 2015in Physical Sciences No comment

There exists an instrument SODI (Selected Optical Diagnostic Instrument) on the ISS where series of the DCMIX (Diffusion Coefficients in Mixtures) experiments are conducted by members of the ESA Topical Team. The study is addressed to the performance of thermal design of SODI instrument for DCMIX configuration. We report the results on the temperature fields which were measured interferometrically both in two ground setups (one thermally optimized; the other one, the engineering model of the ISS SODI-DCMIX experiment: non optimized) and in the ISS experiment itself with the respective numerical simulations. Even though monitoring of the cell with binary mixture THN−nC12 employs only an interferometer with one wave length instead of two for other cells with ternary mixtures, it gives valuable information about the instrument performance. Temperature and concentration fields observed during the tests in the engineering model are compared with those obtained in laboratory experiments with the same liquid, with numerical simulations and with first results from the ISS in Run #16. The thermal design of the microgravity cell, being not optimized for ground experiments, exhibits a promising performance in the weightlessness condition.

Related URLs:
http://dx.doi.org/10.1007/s12217-012-9337-2

Report on Microgravity Experiments of Marangoni Convection Aboard International Space Station

by on 9 June 2015in Physical Sciences No comment

This paper reports some important results obtained from a series of microgravity experiments on the Marangoni convection that takes place in liquid bridges. This project, called Marangoni Experiment in Space (MEIS), started from August 22, 2008 as the first science experiment on the Japanese Experimental Module “KIBO” at the ISS. Two series of experiments, MEIS-1 and 2, were conducted in 2008 and 2009, respectively. The experimental methods used are explained in some detail. The maximum size of the liquid bridge that could be realized during these experiments was 30 mm in diameter and 60 mm in length, giving an aspect ratio of 2.0. The results are obtained for a wide range of aspect ratios of the liquid bridges, including the values that cannot be reached in 1 g experiments, and therefore, they provide indispensable amount of data for the study of instability mechanisms of the Marangoni convection.

Related URLs:
http://dx.doi.org/10.1115/1.4005145

Experimental and numerical analysis of mass transfer in a binary mixture with Soret effect in the presence of weak convection

by on 9 June 2015in Physical Sciences No comment

One of the targets of the experiment IVIDIL (Influence Vibrations on Diffusion in Liquids) conducted on-board ISS was to study the response of binary mixtures to vibrational forcing when the density gradient results from thermal and compositional variations. Compositional variations were created by the Soret effect and can strengthen or weaken the overall density gradient and, consequently, the response to vibrational forcing. We present the results of two experimental runs conducted on-board ISS in the frame of the experiment IVIDIL for low and strong vibrational forcing. The experimental observations revealed that a significant mean flow is set within 2 minutes after imposing vibrations and later in time it varies weakly and slowly due to the Soret effect. A mathematical model has been developed to compute the thermal and concentration fields in the experiment IVIDIL and verify the accuracy of picture processing based on the classical approach used in non-convective systems with the Soret effect. The effect of temperature and concentrations perturbations by joint action of vibrational convection and Soret effect on long time scale are carefully examined. The model demonstrates that image processing used for non-convective systems is suitable for the systems with vibration-affected thermodiffusion experiment.

Related URLs:
http://www.ncbi.nlm.nih.gov/pubmed/25274457

Austrian dose measurements onboard space station MIR and the International Space Station – overview and comparison

by on 9 June 2015in Physical Sciences No comment

The Atominstitute of the Austrian Universities has conducted various space research missions in the last 12 years in cooperation with the Institute for Biomedical Problems in Moscow. They dealt with the exact determination of the radiation hazards for cosmonauts and the development of precise measurement devices. Special emphasis will be laid on the last experiment on space station MIR the goal of which was the determination of the depth distribution of absorbed dose and dose equivalent in a water filled Phantom. The first results from dose measurements onboard the International Space Station (ISS) will also be discussed. The spherical Phantom with a diameter of 35 cm was developed at the Institute for Biomedical Problems and had 4 channels where dosemeters can be exposed in different depths. The exposure period covered the timeframe from May 1997 to February 1999. Thermoluminescent dosemeters (TLDs) were exposed inside the Phantom, either parallel or perpendicular to the hull of the spacecraft. For the evaluation of the linear energy transfer (LET), the high temperature ratio (HTR) method was applied. Based on this method a mean quality factor and, subsequently, the dose equivalent is calculated according to the Q(LET∞) relationship proposed in ICRP 26. An increased contribution of neutrons could be detected inside the Phantom. However the total dose equivalent did not increase over the depth of the Phantom. As the first Austrian measurements on the ISS dosemeter packages were exposed for 248 days, starting in February 2001 at six different locations onboard the ISS. The Austrian dosemeter sets for this first exposure on the ISS contained five different kinds of passive thermoluminescent dosemeters. First results showed a position dependent absorbed dose rate at the ISS.

Related URLs:
http://www.sciencedirect.com/science/article/pii/S0273117704003278